摘要:以钛酸四丁脂、醋酸钡、醋酸镧为原料 ,采用溶胶 -凝胶法制备了掺杂镧BaTiO3 基超细微粉 ,利用DTA、XRD、SEM等测试手段对超细微粉进行了表征。根据Scherrer计算可知 ,超细微粉的粒径在40nm左右
关键词: 溶胶-凝胶法;钛酸钡;纳米晶粉体
Abstract: BaTiO3-based ultra-fine powders doped by lanthanium is prepared by sol-gel process using tetrathoxysilance(TEOS), Mg(NO3) 2·6H2O and Al(NO3) 3·9H2O as raw materials. The structure and compositions of the Ultra-fine powders are characterized by XRD,DTA and SEM.The partical sizes are determined to be 40 nm using Scherrer’s formula.
Keywords:sol-gel process;BaTiO3;nano-powders