高校实验室科学技术
高校实验室科学技术
实验技术与方法
化学实验室中真空系统的三个管理措施
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陈云华*,丁琼,张海波,邓立志,夏春兰
(武汉大学 化学与分子科学学院 湖北, 武汉 430072; 武汉大学 化学国家级实验教学示范中心, 湖北 武汉 430072)
陈云华,男,博士,高级工程师,研究方向为物理化学。Email: chenyh@whu.edu.cn
摘要:
化学实验中很多时候需要使用真空系统。通常情况下,学生实验室采用每一套实验装置配一台真空泵,再附加一些保护装置。这样,搭建一整套真空系统并不简单,而且因同时进行的实验较多,一个实验室配置的真空设备越多,管理难度就越大。本文介绍了3个对化学实验室的真空系统进行改进和改造的方法:①改进真空气路设计,减少真空设备台套数;②改造真空系统设备布置;③防止倒吸返流现象的发生。这些方法可以使之管理起来更方便,同时也改善了实验室环境。
关键词:
化学实验;真空系统;真空气路;共用真空;防止倒吸返流
中图分类号:
G64;O6
基金项目:
Three Management Measures of Vacuum System in Chemical Laboratory
Chen Yunhua*, Ding Qiong, Zhang Haibo, Deng Lizhi, Xia Chunlan
(National Demonstration Center for Experimental Chemistry Education, Wuhan University, Wuhan 430072, China; College of Chemistry and Molecular Sciences, Wuhan University, Wuhan 430072, Hubei, China)
Abstract:
Vacuum is often required in chemical experiments.Usually, the student laboratory uses an experimental apparatus with a vacuum pump and some additional protective devices.Thus, a complete set of vacuum system is not a simple system, and a large number of experiments are performed simultaneously.Therefore, if such a laboratory is equipped with more vacuum equipment, the more difficult it is to manage.This paper introduces the following methods to improve and transform the vacuum system in chemistry laboratory: ①Improve the design of vacuum circuit and reduce the number of vacuum equipment sets;②Upgrade the equipment layout of the vacuum system;③Prevent the occurrence of backflow phenomenon.The vacuum system proposed could make the experiemnt more convenient to manage, also improve the laboratory environment.
KeyWords:
chemical experiments;vacuum system;vacuum circuit;sharing vacuum;prevent backflow